HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 178424321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | N-(4-Amino-o-tolyl)-4-chlorophthalimide | HCID 93991 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178424321 | HCID 178424321 | 148.1% |
Reaction Steps
To a slurry of 150 mg (0.52 mmol) of 2-(4-amino-2-methylphenyl)-5-chlorobenzo[c]azoline-1,3-dione in 2 mL of acetone, was added 41 uL (0.54 mmol) of thiophosgene. The yellow slurry dissolved whereupon a white precipitate formed. After 1 h, this solid was collected by filtration and dried to give 127 mg (74%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08067428B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-78146cea97d8469c867aee23ad5403e4 |
| Source note | uspto-grants-2011_11 |