HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 66995399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl Thioglycolate | HCID 12185 | — |
| Reactant | HCID 86626139 | HCID 86626139 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66995399 | HCID 66995399 | — |
Reaction Steps
Ethyl sulfanylacetate and triethylamine were dissolved in an ethanol solution of 5-[cyano({[(4-methylphenyl)sulfonyl]oxy}imino)methyl]-2-methoxybenzonitrile, followed by stirring for 5 hours under ice-cooling to obtain ethyl 4-amino-3-(3-cyano-4-methoxyphenyl)isothiazole-5-carboxylate. AP: 378.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08067446B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-b27ab6cff85f409fba9256ea96ae214e |
| Source note | uspto-grants-2011_11 |