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3-tert-butyl-1-methyl-1H-pyrazole-5-carboxylic acid → HCID 24810976、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-tert-butyl-1-methyl-1H-pyrazole-5-carboxylic acid | HCID 720529 | — |
| 反応物 | 1-(4-Fluorophenyl)-2-(piperazin-1-yl)ethan-1-one dihydrochloride | HCID 42933716 | — |
| 生成物 | HCID 24810976 | HCID 24810976 | 91.9% |
反応手順
The title compound was prepared in a similar manner as described in Example 1.2, using 3-tert-butyl-1-methyl-1H-pyrazole-5-carboxylic acid (27.3 mg), and 1-(4-fluorophenyl)-2-(piperazin-1-yl)ethanone dihydrochloride (29.5 mg) as starting materials, to afford the title compound (35.5 mg) as a yellow solid. Exact mass calculated for C21H27FN4O2: 386.2. Found: LCMS m/z=387.5 (M+H+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09434692B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-96434d945b19418f81d8c3ae2719b1d7 |
| 出典メモ | uspto-grants-2016_09 |