HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86651109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86651107 | HCID 86651107 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 86651109 | HCID 86651109 | — |
Reaction Steps
(R)-2-(2′-Ethylaminomethyl-5,4′-bis-trifluoromethyl-biphenyl-3-yl)-propionic acid (0.04 g, 0.10 mmol) in MeOH (2 mL) was treated with 2 drops of sulfuric acid at room temperature overnight. The mixture was concentrated, and the crude material was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08067445B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-1424c864a1b540b5aa9c6eda7dc7a1af |
| Source note | uspto-grants-2011_11 |