Phosgene → (3-Chlorophenyl)methyl chloroformate
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH2:5][OH:6].[C:10](Cl)([Cl:12])=[O:11]>>[Cl:12][C:10]([O:6][CH2:5][C:4]1[CH:7]=[CH:8][CH:9]=[C:2]([Cl:1])[CH:3]=1)=[O:11]Participants
3
Procedure
Prepared according to the procedure described in Example 56, Step 1, using the following starting materials: 3-chlorobenzyl alcohol and phosgene (20% in toluene).
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-03bc887913b348aaa1b4fde5cfd3a9ab
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08067445B2
Reaction notes
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