化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
反応手順
A solution of 3-bromo-4-methoxyphenylacetic acid (3.0 g, 12.2 mmol) in EtOH and sulfuric acid was stirred at 100° C. for 2 hours. The mixture was concentrated and partitioned between EtOAc and H2O, and the organic layer was separated to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08067445B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-e3d6e9063a61482c9b1a0e69f21c57b7 |
| 出典メモ | uspto-grants-2011_11 |