Potassium Carbonate → HCID 67007525, compound

Participants

Reaction Steps

3.0 g 2-(3-Bromo-phenylsulfanyl)-propionamide, 1.95 g of 4-carboxybenzene-boronic acid, and 8.05 g potassium carbonate were stirred in a mixture of 25 ml dioxane and 25 ml water. 1.35 g tetrakis-triphenylphosphino-palladium were added under nitrogen atmosphere and the mixture was heated 85 C for 14 hrs. The mixture was diluted with 40 ml water and filtered. The filtrate was adjusted to pH 2 with conc. HCl and the precipitated product isolated by filtration.

Provenance & Evidence