Dimethylamine → HCID 67007525, compound

Participants

Reaction Steps

1.0 g 2 (3-Bromo-phenoxy)-ethyl]-dimethyl-amine, 0.694 g of 4-carboxy-benzeneboronic acid, and 2.86 g potassium carbonate were stirred in a mixture of 5 ml dioxane and 5 ml water. 0.478 g tetrakis-triphenylphosphino-palladium were added under nitrogen atmosphere and the mixture was heated 85 C for 14 hrs. The mixture was diluted with 15 ml water and filtered. The filtrate was adjusted to pH 2 with conc. HCl and the precipitated product isolated by filtration.

Provenance & Evidence