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HRID564271

反应详情

EQUATION

反应方程式

HRID 564271 的结构方程式

REACTANTS

反应物

2
结构：O=C1NC(=O)c2ccccc21.[K]
HCID24194345

未命名化合物

结构：CC(C)(C)OC(=O)/C=C/c1ccn(S(=O)(=O)c2ccc(CBr)cc2)c1
HCID66646385

未命名化合物

2 次

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)/C=C/c1ccn(S(=O)(=O)c2ccc(CN3C(=O)c4ccccc4C3=O)cc2)c1
HCID66646417

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

10 g (E)-3-[1-(4-bromomethyl-benzenesulfonyl)-1H-pyrrol-3-yl]-acrylic acid tert-butyl ester (compound D2) is dissolved in acetone and 6.5 g potassium phthalimide is added and the mixture is stirred for 17.5 h. The suspension is filtered and the product is purified by crystallization.

WORKUP

后处理

  1. filtrationThe suspension is filtered
  2. customthe product is purified by crystallization