(Diethylamino)sulfur trifluoride → HCID 22112574, compound

HRID 564672Notes

Reaction equation

HRID 564672 reaction equation
[CH2:1]([C:9]1[CH:22]=[CH:21][C:20]2[C:19]3[C:14](=[CH:15][C:16]([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])=[CH:17][CH:18]=3)[CH:13](O)[CH2:12][C:11]=2[CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].CCN(S(F)(F)[F:38])CC>ClCCl>[F:38][CH:13]1[CH2:12][C:11]2[CH:10]=[C:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH:22]=[CH:21][C:20]=2[C:19]2[C:14]1=[CH:15][C:16]([CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])=[CH:17][CH:18]=2

Participants

4

Reactant 2

HCID 123472(Diethylamino)sulfur trifluorideHCID 22112586HCID 22112586, compound

Product 1

HCID 22112574HCID 22112574, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

From 2,7-dioctyl-9,10-dihydrophenanthren-9-ol by reaction with DAST in abs. dichloromethane.

Sources & evidence

ORD record
ord-a519817476894e4b91f9d4d0493d56fd
Source dataset
uspto-grants-2001_01
Patent number
US06168838A

Reaction notes

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