(Diethylamino)sulfur trifluoride → HCID 22112579, compound

HRID 564674Notes

Reaction equation

HRID 564674 reaction equation
[CH2:1]([O:7][C:8]1[CH:21]=[CH:20][C:19]2[C:18]3[C:13](=[CH:14][C:15]([O:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])=[CH:16][CH:17]=3)[CH:12](O)[CH2:11][C:10]=2[CH:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].CCN(S(F)(F)[F:36])CC>ClCCl>[F:36][CH:12]1[CH2:11][C:10]2[CH:9]=[C:8]([O:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[CH:21]=[CH:20][C:19]=2[C:18]2[C:13]1=[CH:14][C:15]([O:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])=[CH:16][CH:17]=2

Participants

4

Reactant 2

HCID 123472(Diethylamino)sulfur trifluorideHCID 22112583HCID 22112583, compound

Product 1

HCID 22112579HCID 22112579, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

From 2,7-dihexyloxy-9,10-dihydrophenanthren-9-ol by reaction with DAST in abs. dichloromethane.

Sources & evidence

ORD record
ord-32133b7696f84760b3d9b3bd7d4f8855
Source dataset
uspto-grants-2001_01
Patent number
US06168838A

Reaction notes

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