HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 9-Fluoro-7-(4-hexylphenyl)-2-octyloxyphenanthrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-Hexylphenylboronic Acid | HCID 4197864 | — |
| Reactant | 7-Bromo-9-fluoro-2-octyloxyphenanthrene | HCID 22112584 | — |
| Catalyst | Tetrakis(triphenylphosphine)palladium | HCID 11979704 | — |
| Solvent | Ethanol toluene water | HCID 86587398 | — |
| Product | 9-Fluoro-7-(4-hexylphenyl)-2-octyloxyphenanthrene | HCID 22112587 | — |
Reaction Steps
From 7-bromo-9-fluoro-2-octyloxyphenanthrene by reaction with 4-hexylphenyl-boronic acid, sodium carbonate and tetrakis(triphenylphosphine)palladium(O) in toluene/ethanol/H2O.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06168838A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-f5f58d7160c041bd84f07e4240948f92 |
| Source note | uspto-grants-2001_01 |