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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 564680Generated: October 30, 2026

Sodium Carbonate → 9-Fluoro-7-(2,3-difluoro4-octyloxyphenyl)-2-octyloxyphenanthrene

https://huagongshe.com/reaction/564680

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
Reactant(2,3-Difluoro-4-(octyloxy)phenyl)boronic acidHCID 10850744—
Reactant7-Bromo-9-fluoro-2-octyloxyphenanthreneHCID 22112584—
CatalystTetrakis(triphenylphosphine)palladiumHCID 11979704—
SolventEthanol toluene waterHCID 86587398—
Product9-Fluoro-7-(2,3-difluoro4-octyloxyphenyl)-2-octyloxyphenanthreneHCID 54280078—

Reaction Steps

From 7-bromo-9-fluoro-2-octyloxyphenanthrene by reaction with 2,3-difluoro4-octyloxyphenylboronic acid, sodium carbonate and tetrakis(triphenylphosphine)-palladium (0) in toluene/ethanol/H2O.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06168838A
Source datasetuspto-grants-2001_01
ORD IDord-5da2f766f79d4a14b7538a3f80a8f37d
Source noteuspto-grants-2001_01