HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 9-Fluoro-7-(6-hexyloxypyrid-3-yl)-2-octyloxyphenanthrene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 6-Hexyloxypyridine-3-boronic acid | HCID 22112571 | — |
| Reactant | 7-Bromo-9-fluoro-2-octyloxyphenanthrene | HCID 22112584 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | Ethanol toluene water | HCID 86587398 | — |
| Product | 9-Fluoro-7-(6-hexyloxypyrid-3-yl)-2-octyloxyphenanthrene | HCID 22112572 | — |
Reaction Steps
From 7-bromo-9-fluoro-2-octyloxyphenanthrene by reaction with 6-hexyloxypyridine-3-boronic acid, sodium carbonate and tetrakis(triphenylphosphine)palladium(0) in toluene/ethanol/H2O.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06168838A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-a1275bfe1189467a85a0e45ec835f1ea |
| Source note | uspto-grants-2001_01 |