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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 564682Generated: October 25, 2026

Azobisisobutyronitrile → tert-Butyl methacrylate

https://huagongshe.com/reaction/564682

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
Reactanttert-Butyl methacrylateHCID 11448—
Reactant2-Naphthyl methacrylateHCID 82654—
SolventTolueneHCID 1140—
Producttert-Butyl methacrylateHCID 11448—
ProductNaphthyl methacrylateHCID 4064248—

Reaction Conditions

Temperature70 °C

Reaction Steps

0.3 mol of 2-naphthyl methacrylate and 0.7 mol of tert-butyl methacrylate were mixed with 200 g of toluene, and 2 g of azoisobutylonitrile (AIBN) was added thereto. The mixed system was heated at a temperature of 70° C. for 8 hours and then purified by dropping it into acetone-methanol solvent, to obtain a copolymer of naphthyl methacrylate and tert-butyl methacrylate (Resin A).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06168897A
Source datasetuspto-grants-2001_01
ORD IDord-619dddc516084022b85e8f2c0b3b2efb
Source noteuspto-grants-2001_01