4-(Phenylsulfonyl)aniline → HCID 88216013, compound

HRID 564771Notes

Reaction equation

HRID 564771 reaction equation
[C:1]1([S:7]([C:10]2[CH:16]=[CH:15][C:13]([NH2:14])=[CH:12][CH:11]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:17][C:18]1[C:19]2[CH:27]=[C:26]([Cl:28])[N:25]=[CH:24][C:20]=2[N:21]=[CH:22][N:23]=1>>[ClH:17].[Cl:28][C:26]1[N:25]=[CH:24][C:20]2[N:21]=[CH:22][N:23]=[C:18]([NH:14][C:13]3[CH:15]=[CH:16][C:10]([S:7]([C:1]4[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=4)(=[O:8])=[O:9])=[CH:11][CH:12]=3)[C:19]=2[CH:27]=1

Participants

3

Reactant 2

HCID 5166664-(Phenylsulfonyl)anilineHCID 108218764,6-Dichloropyrido[3,4-d]pyrimidine

Product 1

HCID 88216013HCID 88216013, compound

Procedure

Prepared according to Procedure A from 4-phenylsulphonylaniline (Helv. Chim. Acta., 1983, 66 (4), 1046) and 4,6-dichloropyrido[3,4-d]pyrimidine; δH [2H6]-DMSO 9.09 (1H,s), 8.80-8.88 (2H,m), 8.19 (2H,d), 7.94-8.09 (4H,m), 7.53-7.20 (3H,m); m/z (M+1)+397.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-e8a6b2096e534f6e9b3c9531deb27ecb
Source dataset
uspto-grants-2001_01
Patent number
US06169091A

Reaction notes

Loading…