1,2-Ethanediamine, N1,N1,N2-trimethyl- → HCID 22112832, compound

HRID 564774Notes

Reaction equation

HRID 564774 reaction equation
Cl[C:2]1[N:27]=[CH:26][C:5]2[N:6]=[CH:7][N:8]=[C:9]([NH:10][C:11]3[CH:16]=[CH:15][C:14]([S:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)(=[O:19])=[O:18])=[CH:13][CH:12]=3)[C:4]=2[CH:3]=1.[CH3:28][N:29]([CH3:34])[CH2:30][CH2:31][NH:32][CH3:33]>>[CH3:33][N:32]([C:2]1[N:27]=[CH:26][C:5]2[N:6]=[CH:7][N:8]=[C:9]([NH:10][C:11]3[CH:16]=[CH:15][C:14]([S:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)(=[O:19])=[O:18])=[CH:13][CH:12]=3)[C:4]=2[CH:3]=1)[CH2:31][CH2:30][N:29]([CH3:34])[CH3:28]

Participants

3

Reactant 2

HCID 673381,2-Ethanediamine, N1,N1,N2-trimethyl-HCID 219521656-Chloro-4-(4-phenylsulphonylanilino)pyrido[3,4-d]pyrimidine

Product 1

HCID 22112832HCID 22112832, compound

Procedure

Prepared according to Procedure C from 6-chloro-4-(4-phenylsulphonylanilino)-pyrido[3,4-d]pyrimidine and N,N,N′-trimethylethylenediamine; δH (CDCl3) 8.92 (1H,s), 8.69 (1H,s), 8.49 (1H,s), 7.80-8.05 (6H,m), 7.38-7.60 (3H,m), 6.79 (1H,s), 3.68 (2H,t), 3.42 (3H,s), 2.51 (1H,t), 2.29 (6H,s); m/z (M+1)+463.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-3dc7bf6ea21648229b52438dc310c4da
Source dataset
uspto-grants-2001_01
Patent number
US06169091A

Reaction notes

Loading…