HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 564991Generated: October 31, 2026
Methyl 4-(benzyloxy)-2-methylbenzoate → (4-(Benzyloxy)-2-methylphenyl)methanol
https://huagongshe.com/reaction/564991
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl 4-(benzyloxy)-2-methylbenzoate | HCID 21194710 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (4-(Benzyloxy)-2-methylphenyl)methanol | HCID 23077848 | 0.1% |
Reaction Steps
A suspension of 0.11 g (2.93 mmol) of lithium aluminum hydride in 20 ml of tetrahydrofuran was cooled to 0° C. A solution of 0.75 g (2.93 mol) of methyl 4-benzyloxy-2-methylbenzoate in 20 ml of tetrahydrofuran was added dropwise to the suspension at DOC. After stirring at 0° C. for 2 hours, the reaction mixture was treated in a conventional manner to give 0.66 g of 4-benzyloxy-2-methylbenzyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06169107A |
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| Source dataset | uspto-grants-2001_01 |
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| ORD ID | ord-5c5ee67429b34a8ab831d3b07564fe0c |
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| Source note | uspto-grants-2001_01 |
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