HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(4-benzyloxy-2-methylphenyl)-2-azidopropenoate → 6-benzyloxy-4-methyl-1H-indole-2-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(4-benzyloxy-2-methylphenyl)-2-azidopropenoate | HCID 53708267 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 6-benzyloxy-4-methyl-1H-indole-2-carboxylic acid ethyl ester | HCID 22720009 | — |
Reaction Steps
The reaction was carried out in a manner similar to Reference Example 13 b) except for using 3.22 g of ethyl 3-(4-benzyloxy-2-methylphenyl)-2-azidopropenoate and 100 ml of toluene. Ethyl 6-benzyloxy-4-methyl-2-indolecarboxylate was thus obtained in the yield of 2.66 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06169107A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-90d472811e8e4e1f957263109a124680 |
| Source note | uspto-grants-2001_01 |