HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 21194170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromo-3-methyl-2-nitrophenol | HCID 13088179 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21194170 | HCID 21194170 | — |
Reaction Steps
The reaction was carried out in a manner similar to Reference Example 12 a) except for using 5.11 g (29.9 mmol) of 4-bromo-3-methyl-2-nitrophenol, 6.30 g (27.2 mmol) of benzyl bromide, 8.26 g (59.7 mmol) of potassium carbonate and 150 ml of acetone. 3-Benzyloxy-6-bromo-2-nitrotoluene was thus obtained in the yield of 5.10 g (58.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06169107A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-1b60c91d445648e1b512aedb4905a5dd |
| Source note | uspto-grants-2001_01 |