HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178485129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Guanidine Hydrochloride | HCID 5742 | — |
| Reactant | Methyl 1-methyl-1H-indole-3-carboxylate | HCID 842006 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | HCID 178485129 | HCID 178485129 | 35.9% |
Reaction Steps
The reaction was carried out in a manner similar to Example 1 except for using 1.00 g (5.29 mmol) of methyl 1-methyl-3-indolecarboxylate, 5.05 g (52.9 mmol) of guanidine hydrochloride and 50 ml of a methanol solution of 2.85 g (52.9 mmol) of sodium methoxide. Thus 0.48 g (35.9%) of 1-methyl-3-indoloylguanidine hydrochloride was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06169107A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-f7001c65f3be46fe82e08b468c8e63d2 |
| Source note | uspto-grants-2001_01 |