HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl iodide → HCID 131720074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl iodide | HCID 85247 | — |
| Reactant | HCID 131720075 | HCID 131720075 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131720074 | HCID 131720074 | — |
Reaction Steps
2.5 ml of iodotrimethylsilane are added at 0° to the solution of 7-trimethylsilylamino-3-(3-formyloxy-1-propen-1-yl)-3-cephem-4-carboxylic acid trimethylsilyl ester obtained in Example 2a) in dichloromethane, and the solution is stirred for 4½ hours at 0°. The NMR-spectroscopic data are identical to the data given in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06169180A |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-518478c6a71041e2a823a0b1b3e1d120 |
| Source note | uspto-grants-2001_01 |