HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 9-Acridinecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Acridine-9-carboxylic acid | HCID 94721 | — |
| Product | 9-Acridinecarbonyl chloride | HCID 609960 | — |
Reaction Steps
Thionyl chloride (20 me) was added to 2.2 g of 9-acridinecarboxylic acid, followed by heating under reflux for 5 hours. After the thionyl chloride was distilled off under reduced pressure, 20 ml of methylene chloride were added further. Distillation was repeated twice under reduced pressure, whereby 2.4 g of the compound (2) were obtained (yield: stoichiometric).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06171520B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-04998fb71de94a189b2a007f32bb022c |
| Source note | uspto-grants-2001_01 |