HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15884981, compound → HCID 15884982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15884981 | HCID 15884981 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15884982 | HCID 15884982 | — |
Reaction Steps
A solution of 5-[(benzyl-methyl-amino)-methyl]-6-methyl-1,4-dihydro-quinoxaline-2,3-dione (3.23 g, 10.45 mmol) in DMF (100 mL) was hydrogenated (Pd/C, 20%, 0.5 g) in DMF (100 mL). The suspension was filtered, and the filtrate was evaporated to give a solid, which was crystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172065B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-78888d390d1b4e3d9e5e157ce29b86b8 |
| Source note | uspto-grants-2001_01 |