反应详情

A solution of 2,3-dimethyl-6-nitroaniline (83 g, 500 mmol) in methanol (1000 mL) was hydrogenated (H2, 50 psi) over Raney Nickel (5 g). On completion, the reaction mixture was filtered, and the mother liquor was evaporated to dryness to give a dark solid as the product.

1. filtrationOn completion, the reaction mixture was filtered
2. customthe mother liquor was evaporated to dryness
3. customto give a dark solid as the product