HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11056131, compound → HCID 53756990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11056131 | HCID 11056131 | — |
| Reactant | 2-[4-(Chloromethyl)phenoxy]-N,N-diethylethan-1-amine | HCID 12493691 | — |
| Product | HCID 53756990 | HCID 53756990 | — |
Reaction Steps
2-[4-(2-Diethylamino-ethoxy)-benzyl]-2-(4-methoxy-benzenesulfonyl)-hexanoic acid ethyl ester was prepared according to the general method as outlined in example 12. Starting from 2-(4-methoxy-benzenesulfonyl)-hexanoic acid ethyl ester (4 g, 12.7 mmol) and [2-(4-chloromethyl-phenoxy)-ethyl]-diethylamine (3.38 g, 14 mmol). Yield 8.21 g crude (100%); brown oil; MS: 520.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-d1a6b9ded9a842a79261aab1bffa9ac4 |
| Source note | uspto-grants-2001_01 |