HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)-octanoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Ethyl 2-bromooctanoate | HCID 95580 | — |
| Product | 2-(4-Methoxy-phenylsulfanyl)-octanoic acid ethyl ester | HCID 11438321 | — |
Reaction Steps
2-(4-Methoxy-phenylsulfanyl)-octanoic acid ethyl ester was prepared according to the general method as outlined in example 9. Starting from ethyl 2-bromooctanoate (11.8 g, 47.3 mmol) and 4-methoxythiophenol (6 g, 43 mmol). Yield: 7.24 g (57%); clear oil; MS: 311.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-60c111c317e04feaa32c66df0480a792 |
| Source note | uspto-grants-2001_01 |