HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorothiophenol → HCID 53829634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorothiophenol | HCID 67789 | — |
| Reactant | Ethyl 2-bromooctanoate | HCID 95580 | — |
| Product | HCID 53829634 | HCID 53829634 | — |
Reaction Steps
2-(4-Fluoro-phenylsulfanyl)-octanoic acid ethyl ester was prepared according to the general method as outlined in example 9. Starting from ethyl 2-bromooctanoate (6.47 g, 24.7 mmol) and 4-fluorothiophenol (3 g, 23.4 mmol). Yield: 6.31 g (90%); clear oil; MS: 299 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-ea6dde1122854adbaecea6d712503896 |
| Source note | uspto-grants-2001_01 |