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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 565314Generated: October 29, 2026

HCID 54032112, compound → HCID 53828855, compound

https://huagongshe.com/reaction/565314

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54032112HCID 54032112—
SolventMethanolHCID 887—
SolventSodium HydroxideHCID 14798—
ProductHCID 53828855HCID 53828855—

Reaction Steps

2-(4-Methoxy-benzenesulfonyl)-2-methyl-5-phenyl-pent-4-enoic acid was prepared starting from 2-(4-methoxy-benzenesulfonyl)-2-methyl-5-phenyl-pent-4-enoic acid ethyl ester (3.0 g, 11 mmol) dissolved in methanol (50 ml) and 10 N NaOH (30 ml). The resulting reaction mixture was worked up as outlined in Example 9. Yield 1.9 g, 68%; yellowish oil; MS: 361 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06172057B2
Source datasetuspto-grants-2001_01
ORD IDord-289c946b10244714b4a414db3f36d167
Source noteuspto-grants-2001_01