HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54032112, compound → HCID 53828855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54032112 | HCID 54032112 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 53828855 | HCID 53828855 | — |
Reaction Steps
2-(4-Methoxy-benzenesulfonyl)-2-methyl-5-phenyl-pent-4-enoic acid was prepared starting from 2-(4-methoxy-benzenesulfonyl)-2-methyl-5-phenyl-pent-4-enoic acid ethyl ester (3.0 g, 11 mmol) dissolved in methanol (50 ml) and 10 N NaOH (30 ml). The resulting reaction mixture was worked up as outlined in Example 9. Yield 1.9 g, 68%; yellowish oil; MS: 361 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-289c946b10244714b4a414db3f36d167 |
| Source note | uspto-grants-2001_01 |