HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzyl chloride → 2-[2-hydroxyethyl-[(4-methylphenyl)methyl]amino]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzyl chloride | HCID 7722 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Product | 2-[2-hydroxyethyl-[(4-methylphenyl)methyl]amino]ethanol | HCID 4219208 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(4-methyl-benzyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (4.8 g, 46 mmol) and 4-methylbenzyl chloride (8.5 g, 46 mmol). Yield 9.8 g (99%); MS: 209.9 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-15c5ce3fbfab4545ba2fe37865207da2 |
| Source note | uspto-grants-2001_01 |