HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 11107026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Product | HCID 11107026 | HCID 11107026 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(4-methoxy-benzyl)-amino]-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (12.0 g, 114 mmol) and 4-methoxybenzyl chloride (14.2 g, 100 mmol). Yield 17.5 g, (77%); yellow oil; MS: 226 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-0be627400b7746fbb2eaaaa365df166f |
| Source note | uspto-grants-2001_01 |