HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 9882847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 2-(1H-Indol-3-yl)quinoline-4-carboxylic acid | HCID 22616994 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 9882847 | HCID 9882847 | 95% |
Reaction Steps
To a 10 mL pear-shaped flask was added 2-(3-indolyl)-4-quinolinecarboxylic acid (1 mmol) and 2 mL of acetonitrile followed by a solution of diazomethane (5 mmol) in 2 mL of ether. The reaction mixture was stirred for 1 h and the solvent removed in vacuo to give methyl-2-(3-indolyl)-4-quinolinecarboxylate (95-100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172084B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-49eb8de1ab984efaab9507a07afc4e98 |
| Source note | uspto-grants-2001_01 |