HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 131719708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | 4-Benzylpiperidine | HCID 31738 | — |
| Reactant | 4-(oxiran-2-ylmethoxy)-1H-indole | HCID 605015 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131719708 | HCID 131719708 | — |
Reaction Steps
The title compound was prepared in similar fashion from 4-(oxiranylmethoxy)-1H-indole and 4-phenylmethylpiperidine. The resulting free base was dissolved in ethyl acetate, and precipitated with one equivalent of oxalic acid in ethyl acetate in 52% overall yield. FDMS m/e=364 (M+ of free base). mp 105-107°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172073B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-a1115f96e47d4bba9b6f96ad891b064c |
| Source note | uspto-grants-2001_01 |