HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonylamine → HCID 21268275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonylamine | HCID 2723901 | — |
| Reactant | 6-Chloro-5-methoxy-1H-indole | HCID 13113493 | — |
| Product | HCID 21268275 | HCID 21268275 | — |
Reaction Steps
The title compound was prepared in a fashion similar to that described in Preparation 30 from 6-chloro-5-methoxyindole (2.0 g, 11 mmol) and 4-piperidone hydrochloride hydrate (3.4 g, 22 mmol). The product was isolated as a yellow solid. Yield 2.4 g (83%). mp 222-224° C. FDMS m/e=264 (M+ of free base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172073B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-8f8d2735497f403e844d6a2548c5cd55 |
| Source note | uspto-grants-2001_01 |