4-Piperidineethanol → HCID 22110988, compound

HRID 565656Notes

Reaction equation

HRID 565656 reaction equation
Br[CH2:2][C:3]1([CH3:16])[CH2:7][C:6]2[C:8]([CH3:15])=[C:9]([NH2:14])[C:10]([CH3:13])=[C:11]([CH3:12])[C:5]=2[O:4]1.[NH:17]1[CH2:22][CH2:21][CH:20]([CH2:23][CH2:24][OH:25])[CH2:19][CH2:18]1>>[NH2:14][C:9]1[C:10]([CH3:13])=[C:11]([CH3:12])[C:5]2[O:4][C:3]([CH2:2][N:17]3[CH2:22][CH2:21][CH:20]([CH2:23][CH2:24][OH:25])[CH2:19][CH2:18]3)([CH3:16])[CH2:7][C:6]=2[C:8]=1[CH3:15]

Participants

3

Reactant 2

HCID 739534-PiperidineethanolHCID 108505902-Bromomethyl-2,3-dihydro-2,4,6,7-tetramethyl-5-benzofuranamine

Product 1

HCID 22110988HCID 22110988, compoundYield 88%

Procedure

Using 2-bromomethyl-2,3-dihydro-2,4,6,7-tetramethyl-5-benzofuranamine and 4-piperidineethanol, the procedure of Example 1, presented hereinafter, was otherwise repeated to provide the title compound.

Sources & evidence

ORD record
ord-f5ae5465e40e48d896e5e30603998258
Source dataset
uspto-grants-2001_01
Patent number
US06172085B2

Reaction notes

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