1-Phenethylpiperazine → HCID 22110997, compound

HRID 565695Notes

Reaction equation

HRID 565695 reaction equation
Br[CH2:2][C:3]1([CH3:16])[CH2:7][C:6]2[C:8]([CH3:15])=[C:9]([NH2:14])[C:10]([CH3:13])=[C:11]([CH3:12])[C:5]=2[O:4]1.[C:17]1([CH2:23][CH2:24][N:25]2[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH3:16][C:3]1([CH2:2][N:28]2[CH2:29][CH2:30][N:25]([CH2:24][CH2:23][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[CH2:26][CH2:27]2)[CH2:7][C:6]2[C:8]([CH3:15])=[C:9]([NH2:14])[C:10]([CH3:13])=[C:11]([CH3:12])[C:5]=2[O:4]1

Participants

3

Reactant 2

HCID 792141-PhenethylpiperazineHCID 108505902-Bromomethyl-2,3-dihydro-2,4,6,7-tetramethyl-5-benzofuranamine

Product 1

HCID 22110997HCID 22110997, compoundYield 50%

Procedure

Using 2-bromomethyl-2,3-dihydro-2,4,6,7-tetramethyl-5-benzofuranamine and 1-(2-phenylethyl)piperazine, the procedure of Example 1 was otherwise repeated to provide the title compound.

Sources & evidence

ORD record
ord-f82972a9ce3747c0abeccf01a0d5cee2
Source dataset
uspto-grants-2001_01
Patent number
US06172085B2

Reaction notes

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