HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9959918, compound → HCID 54528448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9959918 | HCID 9959918 | — |
| Solvent | Isopropanol hexane | HCID 21585144 | — |
| Product | HCID 54528448 | HCID 54528448 | — |
Reaction Steps
1-[(5-Amino-2,3-dihydro-2,4,6,7-tetramethylbenzofuran-2-yl)methyl]-N-(diphenylmethyl)-4-piperidinamine was subjected to preparative high-performance liquid chromatography (column: CHIRALCEL OD (20×250 mm, Daicel Chemical Industry, Ltd.), mobile phase: hexane-2-propanol=95:5); flow rate: 80 mL/min., column temperature: 30° C.) to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172085B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-9478e0fad90046a9bf5ebfe986b1c4ac |
| Source note | uspto-grants-2001_01 |