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HRID56572

反应详情

EQUATION

反应方程式

HRID 56572 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(-c2ccco2)cc(OC)c1Br
HCID58431988

未命名化合物

结构：CCOC(C(=O)N(C)OC)c1ccc(-c2nnc(C)o2)cc1
HCID58432091

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(C(=O)c1ccc(-c2cc(OC)c(Br)c(OC)c2)o1)c1ccc(-c2nnc(C)o2)cc1
HCID53378115

未命名化合物

PROCEDURE

实验过程

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)ethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-ethoxy-N-methoxy-N-methyl-2-(4-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (60% EtOAc/hexanes) gave the product as a pale yellow solid (0.070 g, 19% yield). MS: m/z 527.3 [M+H]+.

WORKUP

后处理

  1. customPurification by chromatography (60% EtOAc/hexanes)