Ethanolamine → HCID 22111617, compound

HRID 565732Notes

Reaction equation

HRID 565732 reaction equation
[CH2:1]([CH2:3][NH2:4])[OH:2].[Br:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][S:18](Cl)(=[O:20])=[O:19]>>[OH:2][CH2:1][CH2:3][NH:4][S:18]([CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][Br:5])(=[O:19])=[O:20]

Participants

3

Reactant 2

HCID 700EthanolamineHCID 22111638HCID 22111638, compound

Product 1

HCID 22111617HCID 22111617, compoundYield 73.6%

Procedure

Ethanolamine (0.67 g, 11 mmol) was reacted with 12-bromododecanesulfonyl chloride (1.74 g, 5 mmol) in the same manner as in Preparation Example 4, to give N-(2-hydroxyethyl)-12-bromododecanesulfonamide (1.37 g) as colorless crystals.

Sources & evidence

ORD record
ord-699b4865dc8546a197533a12e4b77367
Source dataset
uspto-grants-2001_01
Patent number
US06172228B2

Reaction notes

Loading…