HRID565737

反应详情

EQUATION

反应方程式

HRID 565737 的结构方程式

PROCEDURE

实验过程

The reaction was carried out in the same manner as in Preparation Example 11 except for using N-methyl-n-butylamine (5.75g, 66 mmol) in place of diethylamine, and 5-chloropentanesulfonyl chloride (6.15g, 30 mmol) in place of 6-chlorohexanesulfonyl chloride in Preparation Example 11, to give N-n-butyl-N-methyl-5-chloropentanesulfonamide (7.12 g) as a pale yellow oil.

WORKUP

后处理

  1. customThe reaction was carried out in the same manner as in Preparation Example 11 except
  2. customin Preparation Example 11