HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → N-cyclopropyl-10-bromodecanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | 10-Bromodecanesulfonyl chloride | HCID 18679845 | — |
| Product | N-cyclopropyl-10-bromodecanesulfonamide | HCID 22111539 | 97.3% |
Reaction Steps
The reaction was carried out in the same manner as in Preparation Example 3 except for using 10-bromodecanesulfonyl chloride (450 mg, 1.41 mmol) in place of 6-bromohexanesulfonyl chloride, and cyclopropylamine (177 mg, 3.10 mmol), to give N-cyclopropyl-10-bromodecanesulfonamide (467 mg) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172228B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-31ac275ffe3b42b1bc5420bd7b949d33 |
| Source note | uspto-grants-2001_01 |