Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 565823Generated: October 29, 2026

Benzaldehyde, 4-(dipropylamino)- → HCID 54100635, compound

https://huagongshe.com/reaction/565823

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehyde, 4-(dipropylamino)-HCID 69171—
ReactantPotassium tert-butoxideHCID 23665647—
ReactantHCID 178476800HCID 178476800—
SolventDimethylformamideHCID 6228—
ProductHCID 54100635HCID 5410063561.6%

Reaction Steps

Using 2.05 g (10.0 mmol) of p-di-n-propylaminobenzaldehyde, 3.6 g (10.9 mmol) of diethyl 3,3-diphenylallylphosphite ((5), R1=R2=H, R=Et), 1.3 g (11.6 mmol) of potassium tert-butoxide, and 15 ml of DMF, the same treatments as in step (5) in Example 1 were performed. Thus, 2.35 g of 1,1-diphenyl-4-(p-di-n-propylaminophenyl)-1,3-butadiene was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06172264B2
Source datasetuspto-grants-2001_01
ORD IDord-fd2da0efbaae48a190da5bc141074bb5
Source noteuspto-grants-2001_01