HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde, 4-(dipropylamino)- → HCID 54100635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde, 4-(dipropylamino)- | HCID 69171 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 178476800 | HCID 178476800 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54100635 | HCID 54100635 | 61.6% |
Reaction Steps
Using 2.05 g (10.0 mmol) of p-di-n-propylaminobenzaldehyde, 3.6 g (10.9 mmol) of diethyl 3,3-diphenylallylphosphite ((5), R1=R2=H, R=Et), 1.3 g (11.6 mmol) of potassium tert-butoxide, and 15 ml of DMF, the same treatments as in step (5) in Example 1 were performed. Thus, 2.35 g of 1,1-diphenyl-4-(p-di-n-propylaminophenyl)-1,3-butadiene was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172264B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-fd2da0efbaae48a190da5bc141074bb5 |
| Source note | uspto-grants-2001_01 |