HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl benzylphosphonate → Benzylphosphonic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl benzylphosphonate | HCID 14122 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Benzylphosphonic Acid | HCID 81312 | 59.2% |
Reaction Steps
A solution of diethyl benzylphosphonate (25 g) in methanol (10 ml) and concentrated hydrochloric acid (500 ml) solution was refluxed for 4 days. The mixture was cooled to room temperature, and precipitated crystal was collected by filtration to give benzylphosphonic acid (11.17 g) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172061B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-dde78dcacfcc4ea3b3cf341bf25c2323 |
| Source note | uspto-grants-2001_01 |