HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nonanone → HCID 72599204, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nonanone | HCID 61235 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 72599204 | HCID 72599204 | — |
Reaction Steps
16.42 g (115 mmol) of 3-nonanone and 15.26 g (115.4 mmol) of tert-butyl carbazate are refluxed for 3 hours in 200 ml of cyclohexane. The solvent is removed in vacuo. This gives 30.54 g (product contains water) of a white solid, Rf=0.49 (cyclohexane/ethyl acetate=3:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174884B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-44ffbfeb61be4a119fd1fc00e4af78ea |
| Source note | uspto-grants-2001_01 |