HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Decanone → tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Decanone | HCID 12203 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Cyclohexane heptane | HCID 21477393 | — |
| Product | tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate | HCID 72599202 | 93% |
Reaction Steps
24.76 g (158 mmol) of 4-decanone and 20.94 g (158 mmol) of tert-butyl carbazate are heated for 90 minutes at 80° C. in 250 ml of cyclohexane/heptane mixture (1:1). After cooling, 39.71 g (93%) of a white solid are obtained by crystallization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174884B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-37087aa4fed64276a09e56a8bf9701c7 |
| Source note | uspto-grants-2001_01 |