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HRID56642

反应详情

EQUATION

反应方程式

HRID 56642 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1cc(Cl)ccc1Cl
HCID2773371

2,5-Dichlorophenylboronic acid

C6H5BCl2O2

结构：CC(C(=O)OC(C)(C)C)n1ccc(Br)cc1=O
HCID117622807

未命名化合物

PRODUCTS

生成物

1
结构：CC(C(=O)OC(C)(C)C)n1ccc(-c2cc(Cl)ccc2Cl)cc1=O
HCID117622663

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccc([P](c2ccccc2)(c2ccccc2)[Pd]([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)[P](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
催化剂HCID178418397

未命名化合物

PROCEDURE

实验过程

2.5 g (8.0 mmol) of tert-butyl 2-(4-bromo-2-oxopyridin-1(2H)-yl)propanoate (racemate) and 1.76 g (9.2 mmol) of 2,5-dichlorophenylboronic acid in the presence of tetrakis(triphenylphosphine)palladium(0) were reacted according to General Method 2A. Yield: 2.3 g (77% of theory)