HCID 21266135, compound → HCID 21266154, compound

Participants

Reaction Steps

4N Hydrochloric acid/ethyl acetate solution (1.58 ml) was added to a solution of {6-[(tetradecylamino)carbonyl]-3-cyclohexenyl}methyl 4-methyltetrahydro-1(2H)-pyrazinecarboxylate (2.500 g) in ethyl acetate (25 ml). After being stirred for 30 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate-ethanol mixed solution, thereby yielding the entitled compound (2.147 g) as white solid.

Provenance & Evidence