HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 86756240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Benzoyl chloride, 3,4-dichloro- | HCID 76403 | — |
| Reactant | HCID 69435312 | HCID 69435312 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86756240 | HCID 86756240 | 29.7% |
Reaction Steps
A mixture of cis and trans 2-benzoyloxymethyl-5-hydroxy-1,3-oxathiolane (as prepared in example 1) (8.99 g, 39.8 mmol) was reacted with 8.3 g (39.6 mmol) of 3,4-dichlorobenzoylchloride in-dichloromethane (30 mL) and pyridine (9.6 mL) as described in Example 2 to yield 4.86 g of the desired compounds in 1:1 ratio.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06175008B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-7b886134901b48258b39e715037f8c1c |
| Source note | uspto-grants-2001_01 |