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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 566547Generated: October 30, 2026

Benzoyl Peroxide → 3-Bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene

https://huagongshe.com/reaction/566547

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoyl PeroxideHCID 7187—
ReactantN-bromobutanimideHCID 67184—
Reactant1-(3-Methoxyphenyl)-1-(2-methylphenyl)-1-propeneHCID 54251528—
SolventCarbon TetrachlorideHCID 5943—
Product3-Bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propeneHCID 53740371—

Reaction Steps

A mixture of 1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene (18.3 g, 0.077 mol), carbon tetrachloride (80 ml), benzoylperoxide (0.15 g) and N-bromosuccinimide (14.2 g, 0.080 mol) was heated at reflux temperature for 5 h. The reaction mixture was left overnight at room temperature, filtered and the filtrate was evaporated in vacuo to give 3-bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene in a quantitative yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06174898B1
Source datasetuspto-grants-2001_01
ORD IDord-05a8794db79440b0833499560acc03c0
Source noteuspto-grants-2001_01