HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 3-Bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1-(3-Methoxyphenyl)-1-(2-methylphenyl)-1-propene | HCID 54251528 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 3-Bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene | HCID 53740371 | — |
Reaction Steps
A mixture of 1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene (18.3 g, 0.077 mol), carbon tetrachloride (80 ml), benzoylperoxide (0.15 g) and N-bromosuccinimide (14.2 g, 0.080 mol) was heated at reflux temperature for 5 h. The reaction mixture was left overnight at room temperature, filtered and the filtrate was evaporated in vacuo to give 3-bromo-1-(3-methoxyphenyl)-1-(2-methylphenyl)-1-propene in a quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174898B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-05a8794db79440b0833499560acc03c0 |
| Source note | uspto-grants-2001_01 |