HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → β,β-Dimethylbenzenepropanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 22346614 | HCID 22346614 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | β,β-Dimethylbenzenepropanamine | HCID 13707364 | — |
Reaction Steps
A mixture of 2,2-dimethyl-3-phenyl-1-azidopropane (3 gm), 10% Pd-C, methanol (60 mL) and tetrahydrofuran (15 mL) was stirred under 1 atmosphere of hydrogen at rt for 18 h. The mixture was filtered and concentrated to give the title compound as an oil, MS (m/z): 164.1 (M+H)+; C11H17N requir. 163.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174901B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-7c7c37ab25c94c708f6b761904902be5 |
| Source note | uspto-grants-2001_01 |